Other Details :
- CSCl2 is prepared in a two-step process from carbon disulfide. In the first step, carbon disulfide is chlorinated to give trichloromethanesulfenyl chloride, CCl3SCl:
- CS2 + 3 Cl2 CCl3SCl + S2Cl2
- The chlorination must be controlled as excess chlorine converts trichloromethanesulfenyl chloride into carbon tetrachloride.
- Steam distillation separates the trichloromethanesulfenyl chloride, a rare sulfenyl chloride, and hydrolyzes the sulfur monochloride.
- Reduction of trichloromethanesulfenyl chloride produces thiophosgene : CCl3SCl + M CSCl2 + MCl2
Red Burgundy Colour
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